2,2,2-三氟乙酸乙酯合成路线 （共 25 条）
反应条件
carbon monoxide in tetrahydrofuran byproducts: Pd(CO)(m)(dpe)n; Addn. of CO (ambient pressure) to metal complex (THF, room temp.), stirring (2 h),; trap-to-trap distn., GLC anal.;
参考文献
Kim, Yong-Joo; Osakada, Kohtaro; Sugita, Kouji; Yamamoto, Takakazu; Yamamoto, Akio
Organometallics, 1988 , vol. 7, p. 2182 - 2188
参考文献
Prakash, G. K. Surya; Mathew, Thomas; Marinez, Eric R.; Esteves, Pierre M.; Rasul, Golam; Olah, George A.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3952 - 3958
参考文献
Bartmess, J. E.; Hays, R. L.; Caldwell, G.
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1338 - 1344
反应条件
in 1,4-dioxane; water T=22°C; pH=12.8; Rate constant;
参考文献
Palling, David J.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4869 - 4876
反应条件
in sulfolane in autoclave; var. solv.: N-methyl-2-pyrrolidone, N,N-dimethylacetamide; Yield given;
参考文献
Shibuta, Daisuke; Watanabe, Masanari; Sato, Kosei
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 176
反应条件
in sulfolane in autoclave; var. solv.: N-methyl-2-pyrrolidone, N,N-dimethylacetamide; Yield given;
参考文献
Shibuta, Daisuke; Watanabe, Masanari; Sato, Kosei
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 176
反应条件
1-n-butyl-3-methylimidazolium chloride in N,N-dimethyl-formamide T=180°C; 3 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Lee, Hyunjoo; Kim, Kyung Hwan; Kim, Honggon; Lee, Sang Deuk; Kim, Hoon Sik
Journal of Fluorine Chemistry, 2004 , vol. 125, # 1 p. 95 - 98
反应条件
in water T=0°C; water content influence; Rate constant;
参考文献
Bentley, T. William; Llewellyn, Gareth; McAlister, J. Anthony
Journal of Organic Chemistry, 1996 , vol. 61, # 22 p. 7927 - 7932
反应条件
Heating; Further byproducts given;
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
反应条件
Heating; Further byproducts given;
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
