2,3-二羟基-4-甲氧基苯甲醛合成路线 （共 29 条）
反应条件
Kochen des Reaktionsprodukts mit Wasser;
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
Full Text Show Details
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1938 , vol. <2> 150, p. 257,260
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in N,N-dimethyl-formamide T=20°C; 18 h; Inert atmosphere;
参考文献
Beale, Thomas M.; Bond, Peter J.; Brenton, James D.; Charnock-Jones, D. Stephen; Ley, Steven V.; Myers, Rebecca M.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 5 p. 1749 - 1759
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=20°C; 3.08333 h;
参考文献
Pettit, George R.; Melody, Noeleen; Thornhill, Andrew; Knight, John C.; Groy, Thomas L.; Herald, Cherry L.
Journal of Natural Products, 2009 , vol. 72, # 9 p. 1637 - 1642
反应条件
potassium carbonate; copper(II) oxide in N,N-dimethyl-formamide 7 h; Heating;
参考文献
Vinogradova, V. I.; Yunusov, M. S.
Chemistry of Natural Compounds, 1985 , vol. 21, # 6 p. 777 - 782
Khimiya Prirodnykh Soedinenii, 1985 , # 6 p. 818 - 823
反应条件
potassium hydroxide; dichloromethane; copper-turnings T=110°C;
参考文献
Campbell et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 1736,1740
反应条件
1: aqueous NaOH; aqueous H2O2 2: ethanol / 100 °C / unter vermindertem Druck und Erhitzen des nach dem Ansaeuern mit wss. Salzsaeure erhaltenen Reaktionsprodukts unter 0,05 Torr View Scheme
参考文献
Cervi, Aymeric; Aillard, Paul; Hazeri, Nourallah; Petit, Laurent; Chai, Christina L. L.; Willis, Anthony C.; Banwell, Martin G.
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9876 - 9882
反应条件
in diethyl ether T=0°C; 1 h; Yields of byproduct given;
参考文献
Singh, Sheo Bux; Pettit, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 17 p. 4105 - 4114
反应条件
potassium carbonate; acetone
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1936 , vol. <2> 145, p. 313,315
反应条件
in diethyl ether T=0°C; 1 h; Yields of byproduct given;
参考文献
Singh, Sheo Bux; Pettit, George R.
Journal of Organic Chemistry, 1989 , vol. 54, # 17 p. 4105 - 4114
反应条件
N,N-diethylaniline T=210 - 215°C; Wittig reaction; 0.25 h;
参考文献
Harayama, Takashi; Katsuno, Keiko; Nishita, Yoshitaka; Fujii, Masako; Abe, Hitoshi; Takeuchi, Yasuo
Heterocycles, 2001 , vol. 54, # 1 p. 319 - 328
