二氢-3-(3-甲基丁基)呋喃-2(3H)-酮合成路线 （共 7 条）
反应条件
hydrogenchloride in water
4 h; HeatingpH=1;
参考文献
Lafont; Cave; Lambrey; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 4 p. 339 - 344
反应条件
1: 60 percent / sodium / ethanol / 3 h / Heating
2: 1) sodium; 2) 7percent aq. H2SO4 / 1) EtOH, reflux, 4 h; 2) H2O
3: 70 percent / sodium hydroxide / H2O / 4 h / 80 °C / pH=14
4: 100 percent / HCl / H2O / 4 h / Heating; pH=1
View Scheme
参考文献
Lafont; Cave; Lambrey; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 4 p. 339 - 344
反应条件
1: 70 percent / sodium hydroxide / H2O / 4 h / 80 °C / pH=14
2: 100 percent / HCl / H2O / 4 h / Heating; pH=1
View Scheme
参考文献
Lafont; Cave; Lambrey; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 4 p. 339 - 344
反应条件
1: 1) sodium; 2) 7percent aq. H2SO4 / 1) EtOH, reflux, 4 h; 2) H2O
2: 70 percent / sodium hydroxide / H2O / 4 h / 80 °C / pH=14
3: 100 percent / HCl / H2O / 4 h / Heating; pH=1
View Scheme
参考文献
Lafont; Cave; Lambrey; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 4 p. 339 - 344
反应条件
potassium hydroxide; ethanol
T=-15°C; Erhitzen des Reaktionsprodukts unter vermindertem Druck;
参考文献
Rothstein
Bulletin de la Societe Chimique de France, 1935 , vol. <5> 2, p. 80,85
反应条件
methanol; platinum
Hydrogenation;
参考文献
Zimmer; Rothe
Journal of Organic Chemistry, 1959 , vol. 24, p. 28,30
反应条件
bei der Destillation unter vermindertem Druck;
参考文献
Bogert; Slocum
Am. Perfumer, vol. 18, p. 626
Chem. Zentralbl., 1925 , vol. 96, # I p. 220
