4-氯-1,8-萘二甲酸酐合成路线 (共 20 条)
反应条件
Cu(OAc)2*2H2O; Mn(II)(OAc)2*2H2O; oxygen; acetic acid; potassium bromide T=100°C;
参考文献
Bukharkina, Tatiana V.; Grechishkina, Olga S.; Digurov, Nikolai G.; Kon'kov, Ivan I.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 394 - 400
反应条件
sodium hydroxide; phosphoric acid; chlorine 3 h; Ambient temperature;
参考文献
Xuhong, Qian; Shengwu, Ren
Journal of Chemical and Engineering Data, 1988 , vol. 33, # 4 p. 528 - 529
反应条件
1: HCl / diethyl ether 2: Na2Cr2O7, AcOH View Scheme
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 36, # 11 p. 1181 - 1182,90 - 91
反应条件
1: aq. NaOH / methanol 2: HCl / diethyl ether 3: Na2Cr2O7, AcOH View Scheme
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 36, # 11 p. 1181 - 1182,90 - 91
反应条件
sodium dichromate; acetic acid T=120°C;
参考文献
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, , vol. <A>, p. 65 - 79
Chem. Zentralbl., , vol. 98, # II p. 426
参考文献
Chem. News J. Ind. Sci., , vol. 98, p. 279
Chem. Zentralbl., , vol. 80, # I p. 1876
反应条件
chloroform; chlorine Behandeln des entstandenen 5-Chlor-acenaphthen mit Natriumdichromat und Eisessig;
参考文献
Chem. News J. Ind. Sci., , vol. 98, p. 279
Chem. Zentralbl., , vol. 80, # I p. 1876
反应条件
sodium dichromate; acetic acid
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 36, # 11 p. 1181 - 1182,90 - 91
参考文献
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, , vol. <A>, p. 420
Chem. Zentralbl., , vol. 100, # I p. 650
反应条件
1: With sodium hydroxide in water T=100°C; 0.0166667 h; microwave irradiation; 2: With mercury(II) diacetate in water T=200°C; Pesci reaction; 0.5 h; microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.25 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Moseley, Jonathan D.; Gilday, John P.
Tetrahedron, 2006 , vol. 62, # 19 p. 4690 - 4697