phosphorus pentachloride das gebildete POCl3 wird abdestilliert;
参考文献
Wegscheider; Furcht
Monatshefte fuer Chemie, 1902 , vol. 23, p. 1126,1128
Full Text Show Details
Limpricht; v. Uslar
Justus Liebigs Annalen der Chemie, 1857 , vol. 102, p. 250,251
in diethyl ether
(N2); addn. of a soln. of ligand in Et2O to a soln. of iron complex in Et2O at room temp., stirring overnight; evapn., dissolving in CH2Cl2, column chromy. (silica gel, CH2Cl2/C6H14 1:1 vol.), recrystn. (CH2Cl2/C6H14); elem. anal.;
参考文献
El-khateeb, Mohammad; Younes, Aseel
Journal of Organometallic Chemistry, 2002 , vol. 664, # 1-2 p. 228 - 233