3-羟基-4-苄氧基苯甲醛合成路线 （共 27 条）
反应条件
1: 86 percent / K2CO3; KI / butan-2-one / 24 h / Heating
2: 86 percent / H2 / Pd/C / ethanol / 2 h / 20 °C
View Scheme
参考文献
Pez, Didier; Leal, Isabel; Zuccotto, Fabio; Boussard, Cyrille; Brun, Reto; Croft, Simon L.; Yardley, Vanessa; Ruiz Perez, Luis M.; Gonzalez Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4693 - 4711
反应条件
1: 86 percent / K2CO3; KI / butan-2-one / 24 h / Heating
2: 86 percent / H2 / Pd/C / ethanol / 2 h / 20 °C
3: 75 percent / K2CO3; KI / acetonitrile / 24 h / Heating
View Scheme
参考文献
Pez, Didier; Leal, Isabel; Zuccotto, Fabio; Boussard, Cyrille; Brun, Reto; Croft, Simon L.; Yardley, Vanessa; Ruiz Perez, Luis M.; Gonzalez Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4693 - 4711
反应条件
1: 86 percent / K2CO3; KI / butan-2-one / 24 h / Heating
2: 86 percent / H2 / Pd/C / ethanol / 2 h / 20 °C
3: 73 percent / K2CO3 / butan-2-one / 24 h / Heating
View Scheme
参考文献
Pez, Didier; Leal, Isabel; Zuccotto, Fabio; Boussard, Cyrille; Brun, Reto; Croft, Simon L.; Yardley, Vanessa; Ruiz Perez, Luis M.; Gonzalez Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4693 - 4711
参考文献
Li, Pixu; Evans, Cory D.; Wu, Yongzhong; Cao, Bin; Hamel, Ernest; Joullie, Madeleine M.
Journal of the American Chemical Society, 2008 , vol. 130, # 7 p. 2351 - 2364
反应条件
triethylamine in tetrahydrofuran
T=20°C; 1 h;
参考文献
SUMITOMO CHEMICAL CO LTD
Patent: JP2005/314352 A, 2005 ;
Location in patent: Page/Page column 59 ;
反应条件
copper(I) bromide in N,N-dimethyl-formamide
2.5 h; Reflux;
参考文献
Vanucci-Bacque, Corinne; Chaabouni, Slim; Fabing, Isabelle; Bedos-Belval, Florence; Baltas, Michel
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 528 - 530
反应条件
1: formic acid; hydroxylamine hydrochloride; sodium formate / 3 h / 125 °C
2: potassium carbonate / N,N-dimethyl-formamide
View Scheme
参考文献
Kumar, Dalip; Patel, Gautam; Vijayakrishnan, Lalitha; Dastidar, Sunanda G.; Ray, Abhijit
Chemical Biology and Drug Design, 2012 , vol. 79, # 5 p. 810 - 818
