1,2,3,4,5-五甲基环戊二烯合成路线 (共 113 条)
反应条件
trifluoroacetic acid
参考文献
White,J.D. et al.
Synthetic Communications, 1973 , vol. 3, p. 425 - 429
反应条件
in methanol Reaction proceeds within seconds at -70°C; Elem. anal. showed admixture of chloride.;
参考文献
Douglas, Trevor; Theopold, Klaus H.
Inorganic Chemistry, 1991 , vol. 30, p. 594 - 596
反应条件
in dichloromethane to benzene soln. decamethylstannocene added more acidic ligand (molar ratio 1:2), stirred for few days; recrystd. from CH3CN, elem. anal.;
参考文献
Kohl, Franz X.; Schlueter, Ewald; Jutzi, Peter
Journal of Organometallic Chemistry, 1983 , vol. 243, # 3 p. C37 - C38
反应条件
in benzene to benzene soln. decamethylstannocene added more acidic ligand (molar ratio 1:1); recrystd. from CH2Cl2, elem. anal.;
参考文献
Kohl, Franz X.; Schlueter, Ewald; Jutzi, Peter
Journal of Organometallic Chemistry, 1983 , vol. 243, # 3 p. C37 - C38
反应条件
oxygen; phenol in various solvent(s) T=92°C; Rate constant;
参考文献
Roth, Wolfgang R.; Hunold, Frank
Liebigs Annalen, 1995 , # 6 p. 1119 - 1122
反应条件
in benzene-d6 under N2, 23°C, color change green-purple-blue;
参考文献
Finke, R. G.; Keenan, S. R.; Watson, P. L.
Organometallics, 1989 , vol. 8, p. 263 - 277
反应条件
in benzene-d6 2 h; Photolysis;
参考文献
Pinkas, Jiri; Cisarova, Ivana; Horacek, Michal; Kubista, Jiri; MacH, Karel
Organometallics, 2011 , vol. 30, # 5 p. 1034 - 1045
反应条件
(i), (ii) I2; Multistep reaction;
参考文献
deVries,L.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1838
反应条件
Nafion-501 in dichloromethane 6 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Childs, Ronald F.; Mika-Gibala, Alicja
Journal of Organic Chemistry, 1982 , vol. 47, # 22 p. 4204 - 4207
参考文献
Diversi, Pietro; Ermini, Luca; Ingrosso, Giovanni; Lucherini, Antonio; Pinzino, Calogero; Sagramora, Laura
Journal of Organometallic Chemistry, 1995 , vol. 494, # 12 p. C1 - C3