1,2,3,4,5-五甲基环戊二烯合成路线 （共 113 条）
反应条件
1: 0.81 g / diethyl ether / 6 h / 25 °C 2: 91 percent Chromat. / H2SO4 / H2O / 0.5 h / Ambient temperature; Irradiation View Scheme
参考文献
Childs, Ronald F.; Zeya, Maung; Dain, Robert P.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 76 - 79
反应条件
in m-xylene T=140°C; 4 h;
参考文献
Pinkas, Jiri; Cisarova, Ivana; Horacek, Michal; Kubista, Jiri; MacH, Karel
Organometallics, 2011 , vol. 30, # 5 p. 1034 - 1045
反应条件
1: K12Ga4[N,N'-bis(2,3-dihydroxybenzoyl)-1,5-diaminonapthalene]6 / D20 / 3 h / 20 °C 2: dipotassium hydrogenphosphate / water-d2; dimethylsulfoxide-d6 / 1 h / 45 °C / pH 8 View Scheme
参考文献
Hastings, Courtney J.; Bergman, Robert G.; Raymond, Kenneth N.
Chemistry - A European Journal, 2014 , vol. 20, # 14 p. 3966 - 3973
反应条件
1: K12Ga4[N,N'-bis(2,3-dihydroxybenzoyl)-1,5-diaminonapthalene]6 / D20 / 3 h / 20 °C 2: dipotassium hydrogenphosphate / water-d2; dimethylsulfoxide-d6 / 1 h / 45 °C / pH 8 View Scheme
参考文献
Hastings, Courtney J.; Bergman, Robert G.; Raymond, Kenneth N.
Chemistry - A European Journal, 2014 , vol. 20, # 14 p. 3966 - 3973
反应条件
1: diethyl ether / -78 - 20 °C 2: benzoic acid / benzene-d6 / 45 °C View Scheme
参考文献
Hastings, Courtney J.; Backlund, Mikael P.; Bergman, Robert G.; Raymond, Kenneth N.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 45 p. 10570 - 10573
反应条件
naphthalene; sodium in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Jutzi, Peter; Holtmann, Udo; Kanne, Dieter; Krueger, Carl; Blom, Richard; et al.
Chemische Berichte, 1989 , vol. 122, p. 1629 - 1640
反应条件
1: HCO2H, H3PO4 2: (i), (ii) I2 View Scheme
参考文献
deVries,L.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1838
反应条件
in benzene T=70°C; 48 h; Inert atmosphere;
参考文献
Ganesamoorthy, Chelladurai; Loerke, Sinah; Gemel, Christian; Jerabek, Paul; Winter, Manuela; Frenking, Gernot; Fischer, Roland A.
Chemical Communications, 2013 , vol. 49, # 28 p. 2858 - 2860
反应条件
oxygen; phenol in various solvent(s) T=71.2°C; P=300.02 Torr; further temperature and O2-pressure; without O2 and phenol; KineticsRate constant;
参考文献
Roth, Wolfgang R.; Hunold, Frank
Liebigs Annalen, 1995 , # 6 p. 1119 - 1122
反应条件
in acetonitrile-D3 (Ar), 2h at 33-82°C; NMR, IR;
参考文献
Kubas, Gregory J.; Kiss, Gabor; Hoff, Carl D.
Organometallics, 1991 , vol. 10, p. 2870 - 2876
