1,2,3,4,5-五甲基环戊二烯合成路线 （共 113 条）
反应条件
C24H14Ga4N2O6(12-)*12K(1+) in water T=50°C; Nazarov cyclization; pH=11; 12 h;
参考文献
Hastings, Courtney J.; Pluth, Michael D.; Bergman, Robert G.; Raymond, Kenneth N.
Journal of the American Chemical Society, 2010 , vol. 132, # 20 p. 6938 - 6940
反应条件
1: in tetrahydrofuran T=0 - 20°C; 3 h; 2: With acetic acid in tetrahydrofuran 3: With hydrogenchloride; water in diethyl ether 0.5 h;
参考文献
FIRMENICH SA
Patent: WO2008/120175 A1, 2008 ;
Location in patent: Page/Page column 13 ;
反应条件
trichloroacetic acid in dichloromethane T=28°C; 1.5 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
trichloroacetic acid in dichloromethane T=28°C; 1.5 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
trichloroacetic acid in dichloromethane T=28°C; 1.5 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
trichloroacetic acid in dichloromethane T=28°C; 1.5 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=110°C; 12 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=110°C; 12 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=110°C; 12 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=110°C; 24 h;
参考文献
Uemura, Minoru; Yagi, Kazunari; Iwasaki, Masayuki; Nomura, Kenichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 15 p. 3523 - 3535
