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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-哌啶甲酸
合成路线
(共 129 条)
636-80-6
2-羧酸吡啶
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
hydrogen; platinum(IV) oxide in water T=60°C; P=3102.9 Torr; 5 h;
参考文献
Shuman, Robert T.; Ornstein, Paul L.; Paschal, Jonathan W.; Gesellchen, Paul D.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 738 - 741
657-27-2
L-赖氨酸盐酸盐
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
hydrogen; palladium on activated carbon in water T=200°C; P=5171.62 Torr; 8 h; Product distribution / selectivity;
参考文献
BOARD OF TRUSTEES OF MICHIGAN STATE UNIVERSITY; MICROBIA, INC.
Patent: WO2008/103366 A2, 2008 ;
Location in patent: Page/Page column 17, 19 ;
98-98-6
2-吡啶甲酸
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
(R)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyldiphenylphosphine; hydrogen; bis(norbornadiene)rhodium(I) tetrafluoroborate in methanol T=60°C; P=75006 Torr; 20 h; Product distribution; Further Variations:ReagentsSolventsratio;
参考文献
Studer, Martin; Wedemeyer-Exl, Christina; Spindler, Felix; Blaser, Hans-Ulrich
Monatshefte fur Chemie, 2000 , vol. 131, # 12 p. 1335 - 1343
56-87-1
赖氨酸
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
cadmium(II) sulphide; sodium sulfate in water 1 h; IrradiationpH 10.1; on titanium(IV) also; stereochemistry of product; tested by FT-IR; Mechanism;
参考文献
Friedrich, Thomas; Zimmermann, Norbert; Stuermer, Rainer
Patent: US2004/158061 A1, 2004 ;
Location in patent: Page 5-6 ;
123811-74-5
4-甲氧基吡啶-2-羧酸盐酸盐
→
反应条件
135607-86-2
+
4043-87-2
2-哌啶甲酸
反应条件
hydrogen; platinum(IV) oxide in ethanol; water T=60°C; P=3102.9 Torr; 24 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shuman, Robert T.; Ornstein, Paul L.; Paschal, Jonathan W.; Gesellchen, Paul D.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 738 - 741
56099-73-1
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
naphthalene; sodium in tetrahydrofuran T=-78°C; 0.75 h;
参考文献
Reddy, Basi V. Subba; Chaya, Dudhmal N.; Yadav, Jhillu S.; Gree, Rene
Synthesis, 2012 , vol. 2012, # 2 p. 297 - 303
115819-92-6
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
hydrogen; palladium on activated charcoal
参考文献
Murahashi, Shun-Ichi; Shiota, Tatsuki
Tetrahedron Letters, 1987 , vol. 28, # 51 p. 6469 - 6472
29547-05-5
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
1: 52 percent / K2CO3 / benzyltriethylammonium chloride / acetonitrile / 20 h / Heating 2: 20percent aq. KOH / methanol / 2 h / Ambient temperature View Scheme
参考文献
Landini, Dario; Penso, Michele
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 420 - 423
620-08-6
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
1: 30percent hydrogen peroxide / acetic acid / 24 h / Heating 2: dimethylcarbamyl chloride / CH2Cl2 / 24 h / Ambient temperature 3: 71 percent / 6 N HCl / 24 h / Heating 4: hydrogen / platinum oxide / ethanol; H2O / 24 h / 60 °C / 3102.9 Torr View Scheme
参考文献
Shuman, Robert T.; Ornstein, Paul L.; Paschal, Jonathan W.; Gesellchen, Paul D.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 738 - 741
1122-96-9
→
反应条件
4043-87-2
2-哌啶甲酸
反应条件
1: dimethylcarbamyl chloride / CH2Cl2 / 24 h / Ambient temperature 2: 71 percent / 6 N HCl / 24 h / Heating 3: hydrogen / platinum oxide / ethanol; H2O / 24 h / 60 °C / 3102.9 Torr View Scheme
参考文献
Shuman, Robert T.; Ornstein, Paul L.; Paschal, Jonathan W.; Gesellchen, Paul D.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 738 - 741
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