3-溴-1-(2-溴乙基)苯合成路线 （共 6 条）
反应条件
phosphorus tribromide T=20°C; 16 h;
参考文献
Blanckaert; Burvenich; Devos; Slegers
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 3 p. 183 - 188
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane T=20°C; 3 h;
参考文献
Molchanov, A. P.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 6.1 p. 935 - 937
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 6 p. 1197 - 1199
参考文献
DePuy; Froemsdorf
Journal of the American Chemical Society, 1957 , vol. 79, p. 3710
反应条件
1: 80 percent / borohydride-tetrahydrofuran complex / 2 h / 20 °C 2: 90 percent / phosphorus tribromide / 16 h / 20 °C View Scheme
参考文献
Blanckaert; Burvenich; Devos; Slegers
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 3 p. 183 - 188
反应条件
tetrabutyl ammonium fluoride in dimethyl sulfoxide T=20°C; 4 h;
参考文献
Berube, Marie; Kamal, Fatima; Roy, Jenny; Poirier, Donald
Synthesis, 2006 , # 18 p. 3085 - 3091
反应条件
caesium carbonate in water; N,N-dimethyl-formamide
1 h; Reflux;
参考文献
Herth, Matthias M.; Hansen, Hanne D.; Ettrup, Anders; Dyssegaard, Agnete; Lehel, Szabolcs; Kristensen, Jesper; Knudsen, Gitte M.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4574 - 4581
