反应条件
1: tetrahydrofuran; toluene / 12 h / Heating 2: 1.) i-Bu2AlH / 1.) hexane, 25 deg C, 16 h, 2.) from 0 to 25 deg C, 3 h 3: 17 percent Spectr. / Et3N, Cl2Pd(PPh3)2, CO / dimethylformamide / 10 h / 100 °C / 30400 Torr View Scheme
参考文献
Negishi, Ei-Ichi; Coperet, Christophe; Ma, Shengming; Mita, Takeshi; Sugihara, Takumichi; Tour, James M.
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5904 - 5918