反应条件
in neat (no solvent) inert atmosphere; 90°C, 1 h; evapn. of HN(SiMe3)2 (reduced pressure), extn. (hexane), filtration, partial evapn. (reduced pressure), crystn. (-20°C, overnight); elem. anal.;
参考文献
Inorganic Chemistry, , vol. 30 - 11, p. 2487 - 2494
