双-[3-(三乙氧基硅)丙基]-四硫化物合成路线 （共 15 条）
反应条件
sodium polysulfide in ethanol T=78°C; Product distribution / selectivity;
参考文献
Frings, Albert; Janssens, Louis; Lotter, Stefan; Deschler, Ulrich; Alig, Alfred
Patent: US2007/66841 A1, 2007 ;
Location in patent: Page/Page column 3-4 ;
反应条件
disodium tetrasulfide in ethanol
参考文献
Krafczyk, Roland; Deschler, Ulrich; Michel, Rudolf
Patent: US2002/10353 A1, 2002 ;
反应条件
Na2S*9H2O; hydrogen sulfide; nitrogen in water; toluene
参考文献
The Goodyear Tire and Rubber Company
Patent: US5405985 A1, 1995 ;
反应条件
sodium sulfide; tetrabutylammomium bromide; sulfur in water T=80 - 90°C; 5.66667 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US2006/106241 A1, 2006 ;
Location in patent: Page/Page column 4 ;
反应条件
NaHS monohydrate; sodium carbonate; sulfur; sodium hydroxide in ethanol; water T=65 - 75°C; Product distribution / selectivity;
参考文献
Korth, Karsten; Kiefer, Ingo; Alig, Alfred; Deschler, Ulrich; Droege, Helmut; Koenigstein, Sefan; Schwan, Stephanie
Patent: US2010/29971 A1, 2010 ;
Location in patent: Page/Page column 10 ;
反应条件
1: With sulfur in toluene T=80°C; 2: With tetrabutylammomium bromide; sulfur in water; toluene T=80 - 85°C; 5.58333 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US2006/106240 A1, 2006 ;
Location in patent: Page/Page column 5 ;
反应条件
1: With sulfur T=80°C; 2: With Na2S3; tetrabutylammomium bromide in water T=80 - 90°C; 3.66667 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US2006/106241 A1, 2006 ;
Location in patent: Page/Page column 3-4 ;
反应条件
sodium oligosulfide in ethylene glycol dimethyl ether 1 h; Heating; Further byproducts given;
参考文献
Yamada, Nobuo; Furukawa, Mutsuhisa; Nishi, Masayuki; Takata, Toshikazu
Chemistry Letters, 2002 , # 4 p. 454 - 455
反应条件
1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
US6777569 B1, ;
Page column 9 ;
反应条件
1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 9 ;
