ClSO2F (sulfuryl chloride fluoride) in dichloromethane
a) -50 deg C, 1 h, b) 20 deg C, 1 h;
参考文献
Dabkowski, Wojciech; Cramer, Friedrich; Michalski, Jan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1447 - 1452
oxalyl difluoride in dichloromethane
cooling in liq. nitrogen --> room temperature, 30 min;
参考文献
Dabkowski, Wojciech; Michalski, Jan; Wasiak, Jacek; Cramer, Friedrich
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 7 p. 817 - 820