反应条件
1: (Z)-7,11-dimethyl-6,10-dodecadien-2-yn-1-ol With bis(cyclopentadienyl)titanium dichloride; chloro-(2-methylpropyl)magnesium in diethyl ether
T=0 - 23°C; 2 h;
2: methyl iodide in tetrahydrofuran
T=0 - 23°C; 2 h; Further stages.;
参考文献
Negishi, Ei-Ichi; Liou, Show-Yee; Xu, Caiding; Huo, Shouquan
Organic Letters, 2002 , vol. 4, # 2 p. 261 - 264