1-甲氧基-2,8,9-三氧杂-5-氮杂-1-硅杂双环[3.3.3]十一烷合成路线 （共 6 条）
反应条件
hydrogenchloride
4 h;
参考文献
Kemmitt, Tim; Henderson, William
Australian Journal of Chemistry, 1998 , vol. 51, # 11 p. 1031 - 1035
反应条件
1: heptafluoroiodopropane / acetonitrile / 0.5 h / 20 °C / Irradiation
2: CH2Cl2 / 1 h / 20 °C / Irradiation
View Scheme
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
1: 15 percent / iodine / CH2Cl2 / -60 °C
2: CH2Cl2 / 1 h / 20 °C / Irradiation
View Scheme
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
in dichloromethane
T=20°C; 1 h; Irradiation; Yield given;
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
in dichloromethane
T=20°C; 0.5 h; Irradiation; Yield given;
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
potassium hydroxide in xylene
参考文献
Voronkov,M.G.; Zelchan,G.I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, # 2 p. 137 - 140
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, # 2 p. 210 - 214
