(3-甲氧基苯基乙炔)三甲基硅烷合成路线 （共 6 条）
反应条件
water; triethylamine; triphenylphosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=160°C; P=51485.6 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 20 p. 5386 - 5392
反应条件
water; triethylamine; triphenylphosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=160°C; P=51485.6 Torr; 4 h;
参考文献
Takeuchi, Ryo; Yasue, Hiroyuki
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5386 - 5392
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Montalbetti, Christian; Savignac, Monique; Bonnefis, Felicie; Genet, Jean Pierre
Tetrahedron Letters, 1995 , vol. 36, # 33 p. 5891 - 5894
反应条件
copper(l) iodide; palladium diacetate; triethylamine; diisopropylamine; [(t-Bu)3PH]BF4
Sonogashira coupling; 24 h; Inert atmosphereReflux;
参考文献
Ladouceur, Sebastien; Soliman, Ahmed M.; Zysman-Colman, Eli
Synthesis, 2011 , # 22 art. no. M79111SS, p. 3604 - 3611
反应条件
triethylamine; palladium diacetate; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt in water; acetonitrile
T=40°C;
参考文献
Montalbetti, Christian; Savignac, Monique; Bonnefis, Felicie; Genet, Jean Pierre
Tetrahedron Letters, 1995 , vol. 36, # 33 p. 5891 - 5894
参考文献
3-Dimensional Pharmaceuticals, Inc.
Patent: US2002/169200 A1, 2002 ;
