1-(4-硝基苯基)丁烷-1,3-二酮合成路线 （共 22 条）
反应条件
sulfuric acid; water; acetic acid
参考文献
Sabnis et al.
Journal of Scientific and Industrial Research, 1958 , vol. 17 A, p. 421,422
参考文献
Hauser; Swamer; Ringler
Journal of the American Chemical Society, 1948 , vol. 70, p. 4023,4025
反应条件
tetrachlorosilane; zinc(II) chloride in dichloromethane
T=25°C; 12 h;
参考文献
Elmorsy, Saad S.; Badawy, Doria S.; Khatab, Tamer K.
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 1 p. 109 - 116
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate
T=77°C;
参考文献
Bartlett, Samuel L.; Beaudry, Christopher M.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9852 - 9855
反应条件
pyridinium chlorochromate in dichloromethane
T=25°C; 6 h;
参考文献
Berti, Federico; Bincoletto, Simone; Donati, Ivan; Fontanive, Giampaolo; Fregonese, Massimo; Benedetti, Fabio
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1987 - 1999
反应条件
dibenzo-18-crown-6; ethanol; sodium hydride in tetrahydrofuran
1.) r.t, 0.5 h, 2.) reflux, 2 h;
参考文献
Popic; Korneev; Nikolaev; Korobitsyna
Synthesis, 1991 , # 3 p. 195 - 198
反应条件
L-proline
T=20°C; 7 h;
参考文献
Shen, Zongxuan; Li, Bin; Wang, Lu; Zhang, Yawen
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8785 - 8788
反应条件
sodium ethanolate in diethyl ether
T=20°C;
参考文献
Sloop, Joseph C.; Boyle, Paul D.; Fountain, Augustus W.; Pearman, William F.; Swann, Jacob A.
European Journal of Organic Chemistry, 2011 , # 5 p. 936 - 941
反应条件
hydrogenchloride in water
T=80°C; 1 h;
参考文献
Korsager, Signe; Nielsen, Dennis U.; Taaning, Rolf H.; Lindhardt, Anders T.; Skrydstrup, Troels
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17687 - 17691
反应条件
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C
1.2: -78 °C
2.1: pyridinium chlorochromate / dichloromethane / 6 h / 25 °C
View Scheme
参考文献
Berti, Federico; Bincoletto, Simone; Donati, Ivan; Fontanive, Giampaolo; Fregonese, Massimo; Benedetti, Fabio
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1987 - 1999
