1-(对甲氧基苯基)-1,3-丁二酮合成路线 (共 26 条)
反应条件
sodium ethanolate 2 h;
参考文献
Davis, Brian R.; Hinds, Mark G.; Ting, Philip P. C.
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 865 - 875
反应条件
samarium (III) iodide in acetonitrile T=-5°C; 3 h;
参考文献
Hao, Wenying; Zhang, Yongmin; Ying, Taokai; Lu, Pin
Synthetic Communications, 1996 , vol. 26, # 12 p. 2421 - 2427
反应条件
dibenzo-18-crown-6; ethanol; sodium hydride in tetrahydrofuran 1.) r.t, 0.5 h, 2.) reflux, 2 h;
参考文献
Popic; Korneev; Nikolaev; Korobitsyna
Synthesis, 1991 , # 3 p. 195 - 198
反应条件
boron trifluoride T=0 - 10°C; Erhitzen des Reaktionsgemisches mit Natriumacetat in Wasser.;
参考文献
Hauser; Swamer; Ringler
Journal of the American Chemical Society, 1948 , vol. 70, p. 4023,4025
Full Text Show Details
Walker; Sanderson; Hauser
Journal of the American Chemical Society, 1953 , vol. 75, p. 4109
反应条件
methanol; water; oxygen; toluene-4-sulfonic acid; palladium dichloride in N,N-dimethyl acetamide T=80°C; P=4560.31 Torr; 10 h; Autoclave; regioselective reaction;
参考文献
Mitsudome, Takato; Yoshida, Syuhei; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 5961 - 5964
Angew. Chem., 2013 , vol. 125, # 23 p. 6077 - 6080,4
反应条件
L-proline T=20°C; 96 h;
参考文献
Shen, Zongxuan; Li, Bin; Wang, Lu; Zhang, Yawen
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8785 - 8788
反应条件
potassium tert-butylate in tert-butyl alcohol T=20°C; 3 h; Inert atmosphere;
参考文献
Nakaiida, Shoho; Kato, Shinzi; Niyomura, Osamu; Ishida, Masaru; Ando, Fumio; Koketsu, Jugo
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 5-6 p. 930 - 946
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; cataCXium®A; caesium carbonate T=60°C; P=2250.23 Torr; 36 h; GloveboxInert atmosphereAutoclave;
参考文献
Schranck, Johannes; Tlili, Anis; Alsabeh, Pamela G.; Neumann, Helfried; Stradiotto, Mark; Beller, Matthias
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12624 - 12628
反应条件
1: NaH / dimethylformamide / 1 h / 27 - 30 °C 2: CuSO4*5H2O / methanol; H2O / 1.5 h / 60 °C View Scheme
参考文献
Mahalingam, Sakkarapalayam M.; Aidhen, Indrapal Singh
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 349 - 351
反应条件
sodium ethanolate in diethyl ether T=0 - 20°C;
参考文献
Allahyari-Devin, Maryam; Abedi, Behnam; Navidpour, Latifeh; Shafiee, Abbas
Journal of the Iranian Chemical Society, 2013 , vol. 10, # 1 p. 43 - 53