2-丙基-1,3,2-苯并二硼烷合成路线 (共 10 条)
反应条件
in toluene stirring (2 h), pptn. on concg.; crystn. (-15°C, 12 h), filtering, drying (vac.);
参考文献
Lantero, Dean R.; Miller, Susanne L.; Cho, Jian-Yang; Ward, Donald L.; Smith III, Milton R.
Organometallics, 1999 , vol. 18, # 2 p. 235 - 247
反应条件
RhCl(PPh3)3 T=20°C; P=750.075 Torr; 3 h;
参考文献
Colin, Sylvie; Vaysse-Ludot, Lucile; Lecouve, Jean-Pierre; Maddaluno, Jacques
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4505 - 4511
反应条件
RhCl(PPh3)3 T=20°C; P=750.075 Torr; 6 h;
参考文献
Colin, Sylvie; Vaysse-Ludot, Lucile; Lecouve, Jean-Pierre; Maddaluno, Jacques
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4505 - 4511
反应条件
in toluene byproducts: propane, propylene; pptn. on stirring (room temp., overnight); washing (toluene), drying (vac.);
参考文献
Lantero, Dean R.; Miller, Susanne L.; Cho, Jian-Yang; Ward, Donald L.; Smith III, Milton R.
Organometallics, 1999 , vol. 18, # 2 p. 235 - 247
参考文献
Gerrard, W.; Mooney, E. F.; Rees, R. G.
Journal of the Chemical Society, 1964 , p. 740 - 745
Full Text Show Details
Gmelin Handbook: B: B-Verb.9, 4.3.1.2, page 135 - 136
参考文献
Gerrard, W.; Mooney, E. F.; Rees, R. G.
Journal of the Chemical Society, 1964 , vol. 1964, p. 740 - 745
Full Text Show Details
Gmelin Handbook: B: B-Verb.9, 5.2.3, page 182 - 189
反应条件
Equilibrium constant;
参考文献
Povie, Guillaume; Villa, Giorgio; Ford, Leigh; Pozzi, Davide; Schiesser, Carl H.; Renaud, Philippe
Chemical Communications, 2010 , vol. 46, # 5 p. 803 - 805
反应条件
Equilibrium constant;
参考文献
Povie, Guillaume; Villa, Giorgio; Ford, Leigh; Pozzi, Davide; Schiesser, Carl H.; Renaud, Philippe
Chemical Communications, 2010 , vol. 46, # 5 p. 803 - 805
反应条件
in benzene-d6 byproducts: catechol;
参考文献
Povie, Guillaume; Villa, Giorgio; Ford, Leigh; Pozzi, Davide; Schiesser, Carl H.; Renaud, Philippe
Chemical Communications, 2010 , vol. 46, # 5 p. 803 - 805
反应条件
Equilibrium constant;
参考文献
Povie, Guillaume; Villa, Giorgio; Ford, Leigh; Pozzi, Davide; Schiesser, Carl H.; Renaud, Philippe
Chemical Communications, 2010 , vol. 46, # 5 p. 803 - 805