1-(3-氟苯基)-1-乙醇合成路线 (共 16 条)
反应条件
1: With (Ph)2SiH2; bis-N-heterocyclic carbene rhodium(III) in toluene T=20°C; 48 h; 2: With hydrogenchloride; methanol in toluene T=20°C; Further stages.;
参考文献
Chen, Tao; Liu, Xu-Guang; Shi, Min
Tetrahedron, 2007 , vol. 63, # 23 p. 4874 - 4880
反应条件
water; sulfuric acid in acetonitrile T=10°C; 1.5 h; Irradiationvar. of catalysts; MechanismRate constantQuantum yield;
参考文献
Wan, Peter; Yates, Keith
Journal of Organic Chemistry, 1983 , vol. 48, # 6 p. 869 - 876
反应条件
(i) Mg, (ii) /BRN= 505984/; Multistep reaction;
参考文献
Choluj, Artur; Kula, Przemyslaw; Dabrowski, Roman; Tykarska, Marzena; Jaroszewicz, Leszek
Journal of Materials Chemistry C, 2014 , vol. 2, # 5 p. 891 - 900
反应条件
1: in carbon disulfide T=20°C; 5 h; 2: With sodium hydroxide; dihydrogen peroxide in methanol; carbon disulfide T=0 - 20°C; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ramachandran, P. Veeraraghavan; Madhi, Sateesh; O'Donnell, Martin J.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 9 p. 1252 - 1255
参考文献
Pfizer Inc
Patent: US6342497 B1, 2002 ;
Location in patent: Page column 32 ;
参考文献
Solomon,I.J.; Filler,R.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3492 - 3496
反应条件
water in acetone T=80°C; Rate constant;
参考文献
Tsuno,Y. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, # 11 p. 3337 - 3346
参考文献
Fukui et al.
Nippon Kagaku Zasshi, 1958 , vol. 79, p. 1428,1430
Chem.Abstr., 1960 , p. 5518
参考文献
Sianesi
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 1749,1759
反应条件
[(2-(benzoimidazol-2-yl)-6-(3,5-dimethylpyrazol-1-yl)pyridine)RuCl2(PPh3)]; potassium tert-butylate; acetone in methanol T=56°C; Oppenauer Oxidation; P=750.075 Torr; 0.05 h; Inert atmosphere; Catalytic behavior;
参考文献
Wang, Qingfu; Du, Wangming; Liu, Tingting; Chai, Huining; Yu, Zhengkun
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1585 - 1588