1: in carbon disulfide T=20°C; 5 h; 2: With hydroxylamine-o-sulphonic acid in methanol; carbon disulfide T=0 - 20°C; 12 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ramachandran, P. Veeraraghavan; Madhi, Sateesh; O'Donnell, Martin J.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 9 p. 1252 - 1255
1: With benzo[1,3,2]dioxaborole; rhodium complex 8 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 5, # 4 p. 1320 - 1330
1: With (R)-1,1'-bis(diphenylphosphino)-2,2'-binapthyl; [Rh(COD)2](1+)*BF4(1-) in ethylene glycol dimethyl ether T=-78 - 20°C; 2: With sodium hydroxide; dihydrogen peroxide in ethylene glycol dimethyl ether T=0 - 20°C; 2 h; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of Fluorine Chemistry, , vol. 128, # 7 p. 827 - 831
