2-(4-(苄氧基)苯基)乙醛合成路线 （共 13 条）
反应条件
1.1: toluene / 20 h / Molecular sieve; Reflux
2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 15.5 h / 0 - 20 °C
2.2: 36 h / 7600.51 Torr
View Scheme
参考文献
Tilley, Andrew J.; Zanatta, Shannon D.; Qin, Cheng Xue; Kim, In-Kyeom; Seok, Young-Mi; Stewart, Alastair; Woodman, Owen L.; Williams, Spencer J.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2353 - 2361
反应条件
1.1: NaHSO3 / ethyl acetate; H2O / 1 h
1.2: 89 percent / H2O / 48 h
2.1: Et3N / diethyl ether
3.1: diethyl ether
4.1: SOBr2; pyridine / toluene / 4 h / 80 °C
View Scheme
参考文献
Aberle, Nicholas; Catimel, Jenny; Nice, Edouard C.; Watson, Keith G.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 13 p. 3741 - 3744
反应条件
1: 84 percent / tetrahydrofuran
2: 94 percent / H2 / 10percent Pd-C / ethanol
View Scheme
参考文献
Takaoka, Eiji; Yoshikawa, Naoki; Yamada, Yoichi M.A.; Sasai, Hiroaki; Shibasaki, Masakatsu
Heterocycles, 1997 , vol. 46, # 1 p. 157 - 163
