2-苯甲酰-2,4-二氯乙酰苯胺合成路线 （共 18 条）
反应条件
in toluene T=10 - 20°C; 3.5 h;
参考文献
Cepanec, Ivica; Litvic, Mladen; Pogorelic, Ivan
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1192 - 1198
反应条件
1: zinc(II) chloride 2: toluene / 0.02 h / |Microwave irradiation View Scheme
参考文献
Singh, Rajesh K.; Prasad; Bhardwaj
Medicinal Chemistry Research, 2013 , vol. 22, # 12 p. 5901 - 5911
反应条件
1: zinc(II) chloride 2: toluene / 0.02 h / |Microwave irradiation View Scheme
参考文献
Singh, Rajesh K.; Prasad; Bhardwaj
Medicinal Chemistry Research, 2013 , vol. 22, # 12 p. 5901 - 5911
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; ammonia in ethanol T=70°C; Further byproducts given;
参考文献
Clarke, George M.; Lee, J. Barry; Swinbourne, Frederick J.; Williamson, Basil
Journal of Chemical Research, Miniprint, 1980 , # 12 p. 4777 - 4793
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; ammonia in ethanol T=70°C; Further byproducts given;
参考文献
Clarke, George M.; Lee, J. Barry; Swinbourne, Frederick J.; Williamson, Basil
Journal of Chemical Research, Miniprint, 1980 , # 12 p. 4777 - 4793
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; ammonia in ethanol T=70°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Clarke, George M.; Lee, J. Barry; Swinbourne, Frederick J.; Williamson, Basil
Journal of Chemical Research, Miniprint, 1980 , # 12 p. 4777 - 4793
反应条件
benzene-1,2-diol; urea; sodium nitrite in N,N-dimethyl-formamide T=20°C; Cyclization; Substitution; 24 h;
参考文献
Ivanov; Grishchuk; Ivanova; Mazepa
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 12 p. 1841 - 1844
反应条件
1: 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; ammonium acetate / ethanol / 6 h / |Reflux 2: dipotassium peroxodisulfate; iodine / acetic acid / 8 h / 65 - 70 °C View Scheme
参考文献
Cepanec, Ivica; Litvic, Mladen; Pogorelic, Ivan
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1192 - 1198
反应条件
1: 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; ammonium acetate / ethanol / 6 h / |Reflux 2: dipotassium peroxodisulfate; iodine / acetic acid / 8 h / 65 - 70 °C 3: sodium hydroxide; water / ethanol / 1.5 h / 5 °C View Scheme
参考文献
Cepanec, Ivica; Litvic, Mladen; Pogorelic, Ivan
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1192 - 1198
反应条件
ammonium hydroxide; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; ammonia in ethanol; water; toluene
