乙酯4-甲氧基苯并基甲酸盐合成路线 （共 31 条）
反应条件
1: With ozone in dichloromethane T=20°C; 2.33333 h; 2: With dimethylsulfide in dichloromethane
参考文献
Gioiello, Antimo; Venturoni, Francesco; Natalini, Benedetto; Pellicciari, Roberto
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3520 - 3523
反应条件
triethylamine tris(hydrogen fluoride) in acetonitrile T=13°C; anodic oxidation;
参考文献
Laurent, Eliane; Marquet, Bernard; Tardivel, Robert
Tetrahedron, 1989 , vol. 45, # 14 p. 4431 - 4444
反应条件
triethylamine tris(hydrogen fluoride) in acetonitrile T=13°C; anodic oxidation;
参考文献
Laurent, Eliane; Marquet, Bernard; Tardivel, Robert
Tetrahedron, 1989 , vol. 45, # 14 p. 4431 - 4444
反应条件
1: With boron trifluoride diethyl etherate in acetonitrile T=20°C; 2: With ozone in dichloromethane T=20°C; 2.33333 h; 3: With dimethylsulfide in dichloromethane
参考文献
Gioiello, Antimo; Venturoni, Francesco; Natalini, Benedetto; Pellicciari, Roberto
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3520 - 3523
反应条件
1.1: t-BuOK / tetrahydrofuran / 0.25 h / 0 °C 2.1: β-AD-mix; (DHQD)2PHAL; methanesulfonamide / H2O; 2-methyl-propan-2-ol / 0 °C 2.2: sodium sulfite; H2O / 2-methyl-propan-2-ol / 0.75 h / 0 - 20 °C View Scheme
参考文献
Monenschein, Holger; Draeger, Gerald; Jung, Alexander; Kirschning, Andreas
Chemistry - A European Journal, 1999 , vol. 5, # 8 p. 2270 - 2280
反应条件
aluminium trichloride in chloroform T=0 - 5°C; 1.33333 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Itoh, Osamu; Nagata, Takayoshi; Nomura, Isamu; Takanaga, Tetsuya; Sugita, Toshio; Ichikawa, Katsuhiko
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 810 - 814
反应条件
aluminium trichloride in dichloromethane T=0 - 5°C; 1.33333 h; modification without solvent (other time); Title compound not separated from byproducts;
参考文献
Itoh, Osamu; Nagata, Takayoshi; Nomura, Isamu; Takanaga, Tetsuya; Sugita, Toshio; Ichikawa, Katsuhiko
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 810 - 814
反应条件
1: 71 percent / BTAC / CH2Cl2; H2O / 20 °C 2: 64 percent / LDA / tetrahydrofuran / -78 - 20 °C View Scheme
参考文献
Adlerova,E. et al.
Collection of Czechoslovak Chemical Communications, 1964 , vol. 29, p. 97 - 120
反应条件
dimethylsulfide; oxygen; ozone 1) MeOH, -78 deg C; 2) room temp.; Yield given. Multistep reaction;
参考文献
Kwon, Hyok Boong; McKee, Blain H.; Stille, J. K.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3114 - 3118
反应条件
magnesium 1.) THF, 2.) -50 deg C up to room temp. within 3h; Yield given. Multistep reaction;
参考文献
Nimitz, Jonathan S.; Mosher, Harry S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 211 - 213
