1: With n-butyllithium; N,N,N'-trimethyl-ethylenediamine in tetrahydrofuran; hexane T=-20 - -7°C; 24.5 h; Inert atmosphere; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere; 3: With hydrogenchloride in tetrahydrofuran; hexane; water 0.5 h; Reflux;

N,N-dimethyl-N-(4'-methylphenyl)amine N-oxide in dichloromethane T=20°C; 0.0166667 h;

tetrakis(triphenylphosphine) palladium(0); caesium carbonate in ethanol; toluene T=150°C; Suzuki-Miyaura coupling /aldol condensation reaction; P=4500.45 - 6000.6 Torr; 0.166667 h; Microwave irradiationInert atmosphere;