water

in tetrahydrofuran; water T=65°C; 2 h;

Stage #1: <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4122952', constants.ctx, '0')">sodium hydride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />&nbsp;RefluxInert atmosphere;&nbsp;<br />Stage #2: <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1697092', constants.ctx, '0')">tert-butylhypochlorite</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-30 - 0&deg;C;&nbsp;4&nbsp;h;&nbsp;&nbsp;Darkness;&nbsp;<br /> &nbsp;