N-(4-溴苯基)邻苯二甲酰亚胺合成路线 (共 13 条)
反应条件
N,N-dimethyl-formamide 0.00416667 h; microwave irradiation;
参考文献
Mogilaiah; Reddy, G. Randheer
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 4 p. 882 - 884
反应条件
1,3-bis-(diphenylphosphino)propane; palladium diacetate; caesium carbonate in toluene T=95°C; 24 h;
参考文献
Worlikar, Shilpa A.; Larock, Richard C.
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7175 - 7180
反应条件
triphenylphosphine in neat (no solvent) T=120°C; Aza-Wittig Reaction; 0.5 h; Green chemistry;
参考文献
Sathishkumar, Murugan; Palanikumar, Kulandaivel; Mariappan, Arumugam; Archana, Sivasubramaniyan; Ponnuswamy, Alagusundaram
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 5 p. 681 - 685
反应条件
1H-imidazole; N,N-dimethyl-formamide in neat (no solvent) T=150°C; 3 h;
参考文献
Neves Filho, Ricardo A. W.; Palm-Forster, Mieder A. T.; De Oliveira, Ronaldo N.
Synthetic Communications, 2013 , vol. 43, # 11 p. 1571 - 1576
反应条件
acetyl chloride T=52°C; 2.5 h; Yield given;
参考文献
Kumar, Padam Praveen; Rama Devi; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1166 - 1171
反应条件
in N,N-dimethyl acetamide 0.05 h;
参考文献
Khajavi, Mohammad S.; Nikpour, Farzad; Hajihadi, Mostafa
Journal of Chemical Research - Part S, 1996 , # 2 p. 96 - 97
反应条件
1: toluene-4-sulfonic acid / neat (no solvent, solid phase) / 0.08 h / |Milling; |Green chemistry 2: dicyclohexyl-carbodiimide / neat (no solvent, solid phase) / |Milling; |Green chemistry View Scheme
参考文献
Knoelker, Hans-Joachim; Reddy, Kethiri R.
Synlett, 1999 , # 5 p. 596 - 598
反应条件
1: toluene-4-sulfonic acid / neat (no solvent, solid phase) / 0.08 h / |Milling; |Green chemistry 2: dicyclohexyl-carbodiimide / neat (no solvent, solid phase) / |Milling; |Green chemistry View Scheme
参考文献
Knoelker, Hans-Joachim; Reddy, Kethiri R.
Synlett, 1999 , # 5 p. 596 - 598
反应条件
tetrabutylammomium bromide in neat (no solvent, solid phase) MillingGreen chemistry;
参考文献
Kumar, Padam Praveen; Rama Devi; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1166 - 1171
反应条件
tri-tert-butyl phosphine; [bis(acetoxy)iodo]benzene; palladium diacetate T=100°C; 33 h; Inert atmosphereGlovebox; Overall yield = 82 percent; Overall yield = 247 mg;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483