3,3′-二甲氧基苯偶酰合成路线 （共 20 条）
反应条件
ammonium nitrate; chloro-trimethyl-silane; copper diacetate; Li-naphthalenide Yield given. Multistep reaction;
参考文献
BIOENERGENIX; McCall, John M.; Romero, Donna L.
Patent: US2014/128392 A1, 2014 ;
反应条件
1: Grubb's 2nd generation catalyst / toluene / 1.5 h / 80 °C / |Inert atmosphere 2: Grubb's 2nd generation catalyst; tetra-(n-butyl)ammonium iodide; tert.-butylhydroperoxide / toluene; acetonitrile; water / 1 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
反应条件
1: sulfuric acid / water 2: naphthalene; chloro-trimethyl-silane / water; tetrahydrofuran View Scheme
参考文献
BIOENERGENIX; McCall, John M.; Romero, Donna L.
Patent: US2014/128392 A1, 2014 ;
反应条件
in toluene Heating; Yields of byproduct given;
参考文献
Cameron, James F.; Willson, C. Grant; Frechet, Jean M. J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2429 - 2442
反应条件
1: alcohol; potassium cyanide 2: diluted alcohol / durch Einwirkung von Fehlingscher Loesung View Scheme
参考文献
Schoenberg; Malchow
Chemische Berichte, 1922 , vol. 55, p. 3750
反应条件
carbon monoxide; sodium methylate; methyl iodide; N-hexadecyl-N,N,N-trimethylammonium bromide T=20°C; 20 h;
参考文献
Miura, Masahiro; Akase, Fumiaki; Shinohara, Masato; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1021 - 1026
反应条件
1: aqueous HCl; toluene; amalgamated zinc / Hydrierung der Reaktionsprodukte in Aethanol an Raney-Nickel
2: glacial acetic acid; aqueous HI
View Scheme
参考文献
Cornforth; Robinson
Journal of the Chemical Society, 1942 , p. 684,687
反应条件
sodium dithionite; sodium carbonate; racemic thiourea-based bifunctional organocatalyst in diethyl ether; water
T=20°C; 48 h;
参考文献
Procuranti, Barbara; Connon, Stephen J.
Chemical Communications, 2007 , # 14 p. 1421 - 1423
反应条件
pyridine hydrochloride
T=200°C;
参考文献
Jester, Stefan-S.; Sigmund, Eva; Roeck, Lisa M.; Hoeger, Sigurd
Angewandte Chemie - International Edition, 2012 , vol. 51, # 34 p. 8555 - 8559
反应条件
potassium phosphate; oxygen; copper diacetate; p-toluidine; sodium sulfate in dimethyl sulfoxide
T=140°C; 6 h; Sealed tube;
参考文献
Maji, Arun; Rana, Sujoy; Akanksha; Maiti, Debabrata
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2428 - 2432
Angew. Chem., 2014 , vol. 126, # 9 p. 2460 - 2464,5
