(S)-1-氨基丙烷-2-氨基甲酸苄酯合成路线 (共 5 条)
反应条件
hydrogenchloride; triphenylphosphine in tetrahydrofuran
参考文献
Alongi, Maddalena; Minetto, Giacomo; Taddei, Maurizio
Tetrahedron Letters, 2005 , vol. 46, # 41 p. 7069 - 7072
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=-10°C;
参考文献
Sureshbabu, Vommina V.; Naik, Shankar A.; Hemantha; Narendra; Das, Ushati; Guru Row, Tayur N.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5260 - 5266
反应条件
1: MsCl; NaN3; TBAI / toluene / 6 h / 80 °C
2: 81 percent / PPh3; aq. HCl / tetrahydrofuran
View Scheme
参考文献
Alongi, Maddalena; Minetto, Giacomo; Taddei, Maurizio
Tetrahedron Letters, 2005 , vol. 46, # 41 p. 7069 - 7072
反应条件
dimethylsulfide borane complex in tetrahydrofuran; dichloromethane
24.3333 h; RefluxInert atmosphere;
参考文献
Xu, Zhigang; DiCesare, John C.; Baures, Paul W.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 248 - 254
反应条件
in ethanol
T=0 - 20°C; 18 h;
参考文献
Sugiyama, Toru; Imamura, Yasutada; Demizu, Yosuke; Kurihara, Masaaki; Takano, Masashi; Kittaka, Atsushi
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 24 p. 7317 - 7320