二油酰基 L-α-磷脂酰乙醇胺合成路线 (共 7 条)
反应条件
PLD transesterification;
参考文献
Harris; Marshall; Lee; Siegel; Mcneilly; Yew; Nietupski; Nichols; Cherry; Wan; Jiang; Lane; Rowe; Scheule; Smith; Cheng
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 289 - 292
反应条件
1: 84 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / CH2Cl2; H2O / 2 h 2: 1) Et3N, POCl3, 2) Et3N / 1) THF, a) 0 deg C, 1 h, b) room temp., 3 h, 2) THF, a) 0 deg C, 4 h, b) room temp., 8 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 74, # 8 p. 1697 - 1706
反应条件
triethylamine; trichlorophosphate 1) THF, a) 0 deg C, 1 h, b) room temp., 3 h, 2) THF, a) 0 deg C, 4 h, b) room temp., 8 h; Yield given. Multistep reaction;
参考文献
Helvetica Chimica Acta, , vol. 74, # 8 p. 1697 - 1706
反应条件
1: 66 percent 2: 80 percent 3: 90 percent / PLD View Scheme
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 109, # 1-4 p. 289 - 292
反应条件
1: 80 percent 2: 90 percent / PLD View Scheme
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 109, # 1-4 p. 289 - 292
反应条件
1: (i) NaI, (ii) AgNO3 2: benzene 3: (i) NaI, (ii) aq. AcOH View Scheme
参考文献
Journal of the Chemical Society. Perkin transactions 1, , vol. 12, p. 1404 - 1412
反应条件
acetic acid; platinum Hydrogenation;
参考文献
Baer; Buchnea
Journal of the American Chemical Society, 1959 , vol. 81, p. 1758,1761