2,6-二甲基-4-(3-硝基苯基)吡啶合成路线 （共 9 条）
反应条件
1.5 h; Heatingheating in Dowterm;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 96 percent / 4N aq. HNO3 / 1 h / Heating
2: 82 percent / NaOH / aq. ethanol / 2 h / Heating
3: 99 percent / 1.5 h / Heating; heating in Dowterm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 80 percent / conc. aq. ammonium hydroxide / methanol / 4 h / Heating
2: 96 percent / 4N aq. HNO3 / 1 h / Heating
3: 82 percent / NaOH / aq. ethanol / 2 h / Heating
4: 99 percent / 1.5 h / Heating; heating in Dowterm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 82 percent / NaOH / aq. ethanol / 2 h / Heating
2: 99 percent / 1.5 h / Heating; heating in Dowterm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
sulfuric acid; nitric acid
T=65 - 70°C;
参考文献
Emmert; Diefenbach; Eck
Chemische Berichte, 1927 , vol. 60, p. 2217,2221
反应条件
sulfuric acid; nitric acid
T=0°C; 3 h;
参考文献
Prostakov, N. S.; Soldatenkov, A. T.; Krapivko, A. P.; Fomichev, A. A.; Mikaya, A. I.; Ustenko, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 958 - 963
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1106 - 1113
反应条件
sulfuric acid; nitric acid; phosphorus trichoride
1.)100 deg C, 12 h 2.)CHCl3, 60 deg C, 2 h; Multistep reaction;
参考文献
Prostakov, N. S.; Soldatenkov, A. T.; Krapivko, A. P.; Fomichev, A. A.; Mikaya, A. I.; Ustenko, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 958 - 963
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1106 - 1113
反应条件
1: 100 percent / aq. H2O2, 30percent / acetic acid / 3 h / Heating
2: 0.5 h / Heating
3: conc. HCl / 1 h / Heating
4: 76 percent / activated manganese dioxide / CHCl3 / 6 h / Heating
5: 95 percent / palladium on charcoal / various solvent(s) / 1 h / 190 °C / heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
hydrogen; palladium on activated charcoal in N,N-dimethyl-formamide
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
