[[[3-(2,6-二甲基-4-吡啶基)苯基]氨基]亚甲基]丙二酸二乙酯合成路线 (共 4 条)
反应条件
T=130°C; 0.133333 h;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
2: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
2: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
3: 24 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
in various solvent(s)
0.2 h; Heatingheating in Dowtherm;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863