3-(2,6-二甲基-4-吡啶基)苯胺合成路线 （共 9 条）
反应条件
hydrogen; palladium on activated charcoal in N,N-dimethyl-formamide
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 96 percent / 4N aq. HNO3 / 1 h / Heating
2: 82 percent / NaOH / aq. ethanol / 2 h / Heating
3: 99 percent / 1.5 h / Heating; heating in Dowterm
4: 82 percent / H2 / palladium on charcoal / dimethylformamide
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 80 percent / conc. aq. ammonium hydroxide / methanol / 4 h / Heating
2: 96 percent / 4N aq. HNO3 / 1 h / Heating
3: 82 percent / NaOH / aq. ethanol / 2 h / Heating
4: 99 percent / 1.5 h / Heating; heating in Dowterm
5: 82 percent / H2 / palladium on charcoal / dimethylformamide
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 99 percent / 1.5 h / Heating; heating in Dowterm
2: 82 percent / H2 / palladium on charcoal / dimethylformamide
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 82 percent / NaOH / aq. ethanol / 2 h / Heating
2: 99 percent / 1.5 h / Heating; heating in Dowterm
3: 82 percent / H2 / palladium on charcoal / dimethylformamide
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 78 percent / 0.13 h / 130 °C
2: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
3: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 78 percent / 0.13 h / 130 °C
2: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
3: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
4: 24 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 78 percent / 0.13 h / 130 °C
2: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
T=130°C; 0.133333 h;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
