7-(2,6-二甲基-4-吡啶基)-1-乙基-1,4-二氢-4-氧代喹啉-3-羧酸合成路线 (共 4 条)
反应条件
1: 78 percent / 0.13 h / 130 °C
2: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
3: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
4: 24 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 85 percent / various solvent(s) / 0.2 h / Heating; heating in Dowtherm
2: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
3: 24 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
1: 65 percent / 1) potassium carbonate / dimethylformamide / 1) 60 deg C, 15 min; 2) stirring 1 h;
2: 24 percent / aq. 10percent KOH / 1 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863
反应条件
potassium hydroxide
1 h; Heating;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1857 - 1863