苄基-((E)-3-苯基-烯丙基)-胺合成路线 （共 35 条）
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; (S)-(1,1'-binaphthalene-2,2'-dioxy)P(N(R)-CH(o-Tol)Me)2 in tetrahydrofuran
T=20°C; 16 h; Product distribution; Further Variations:Reagents;
参考文献
Tissot-Croset, Kanne; Polet, Damien; Alexakis, Alexandre
Angewandte Chemie - International Edition, 2004 , vol. 43, # 18 p. 2426 - 2428
反应条件
C28H29N2PdS(1+)*BF4(1-) in tetrahydrofuran
T=50°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Krishnan, Deepa; Wu, Meiyi; Chiang, Minyi; Li, Yongxin; Leung, Pak-Hing; Pullarkat, Sumod A.
Organometallics, 2013 , vol. 32, # 8 p. 2389 - 2397
反应条件
1: 100 percent / Ph3P; DIAD / tetrahydrofuran / 1 h / 20 °C
2: 88 percent / mercaptoacetic acid; Et3N / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Blid, Jan; Brandt, Peter; Somfai, Peter
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3043 - 3049
反应条件
in dichloromethane
36 h; Ambient temperature;
参考文献
Nakanishi, Saburo; Okamoto, Kenji; Yamaguchi, Hiroshi; Takata, Toshikazu
Synthesis, 1998 , # 12 p. 1735 - 1741
反应条件
PPA in chloroform
T=150 - 170°C; 2 h;
参考文献
Euerby, Melvin R.; Waigh, Roger D.
Journal of Chemical Research, Miniprint, 1987 , # 2 p. 554 - 575
反应条件
1: methanol / 3 h / Ambient temperature
2: NaBH4 / methanol / 0.25 h / Ambient temperature
View Scheme
参考文献
Abdel-Magid, Ahmed F.; Carson, Kenneth G.; Harris, Bruce D.; Maryanoff, Cynthia A.; Shah, Rekha D.
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3849 - 3862
反应条件
1.1: NaH / dimethylformamide; various solvent(s) / 0.33 h / 20 °C
1.2: dimethylformamide; various solvent(s) / 16.5 h / 20 °C
1.3: aq. HCl / dimethylformamide; various solvent(s) / 3 h / 20 °C
2.1: 82 mg / toluene / 3 h / Heating
View Scheme
参考文献
Bower, John F.; Chakthong, Suda; Venda, Jakub; Williams, Andrew J.; Lawrence, Ron M.; Szeto, Peter; Gallagher, Timothy
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 10 p. 1868 - 1877
反应条件
in diethyl ether
1.) 1 h, reflux, 2.) r.t., overnight;
参考文献
Euerby, Melvin R.; Waigh, Roger D.
Journal of Chemical Research, Miniprint, 1987 , # 2 p. 554 - 575
反应条件
potassium tert-butylate in tetrahydrofuran
Ambient temperature; Yield given;
参考文献
Evans, Paul; Taylor, Richard J. K.
Synlett, 1997 , vol. 1997, # 9 p. 1043 - 1044
反应条件
1: 78 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 24 h / Ambient temperature
2: lithium aluminum hydride / diethyl ether / Heating
View Scheme
参考文献
Kathryn, E. Bell; Knight, David W.; Gravestock, Michael B.
Tetrahedron Letters, 1995 , vol. 36, # 47 p. 8681 - 8684
