三氟甲基亚磺酸锌(II)合成路线 （共 11 条）
反应条件
tert.-butylhydroperoxide; IPS; zinc sulfinate in water; dimethyl sulfoxide T=20 - 50°C; 12 h; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 135, # 32 p. 12122 - 12134
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.4.2, page 117 - 172
反应条件
tert.-butylhydroperoxide; IPS; zinc sulfinate in chloroform; water T=20 - 50°C; 12 h; Overall yield = 48 percent; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 135, # 32 p. 12122 - 12134
反应条件
tert.-butylhydroperoxide; IPS; zinc sulfinate in chloroform; water T=20 - 50°C; 12 h; regioselective reaction;
参考文献
O'Hara, Fionn; Blackmond, Donna G.; Baran, Phil S.
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 12122 - 12134
反应条件
tert.-butylhydroperoxide in dichloromethane; water T=25°C;
参考文献
Fujiwara, Yuta; Dixon, Janice A.; O'Hara, Fionn; Funder, Erik Daa; Dixon, Darryl D.; Rodriguez, Rodrigo A.; Baxter, Ryan D.; Herle, Bart; Sach, Neal; Collins, Michael R.; Ishihara, Yoshihiro; Baran, Phil S.
Nature, 2012 , vol. 491, # 7427 p. 95 - 99
反应条件
tert.-butylhydroperoxide in dichloromethane; water T=25°C;
参考文献
Nature, , vol. 491, # 7427 p. 95 - 99
反应条件
tert.-butylhydroperoxide in dichloromethane; water T=25°C; Overall yield = 35 percent;
参考文献
Nature, , vol. 491, # 7427 p. 95 - 99
反应条件
tert.-butylhydroperoxide; IPS; zinc sulfinate in chloroform; water T=20 - 50°C; 12 h; Overall yield = 53 percent; Overall yield = 15.7 mg; regioselective reaction;
参考文献
O'Hara, Fionn; Blackmond, Donna G.; Baran, Phil S.
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 12122 - 12134
反应条件
tert.-butylhydroperoxide; IPS; zinc sulfinate in chloroform; water T=20 - 50°C; 20 h; Overall yield = 39 percent; Overall yield = 43 percentSpectr.; regioselective reaction;
参考文献
O'Hara, Fionn; Blackmond, Donna G.; Baran, Phil S.
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 12122 - 12134
反应条件
tert.-butylhydroperoxide; IPS; zinc sulfinate in chloroform; water
T=20 - 50°C; 12 h; Overall yield = 23 percent; regioselective reaction;
参考文献
O'Hara, Fionn; Blackmond, Donna G.; Baran, Phil S.
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 12122 - 12134
