2-(3-氯苯基硫代)乙酸合成路线 (共 8 条)
反应条件
ammonium cerium(IV) nitrate in water; acetic acid T=25 - 45°C; ΔH(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Gurumurthy, Rajagopala; Gopalakhrishnan, Mannathusamy; Sathiyanarayanan, Kulathu Iyer
Tetrahedron, 1994 , vol. 50, # 48 p. 13731 - 13738
反应条件
perchloric acid; NaBO3; acetic acid T=24.9°C; var. temp., ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataMechanism;
参考文献
Kabilan, S.; Pandiarajan, K.; Krishnasamy, K.; Sankar, P.
International Journal of Chemical Kinetics, 1995 , vol. 27, # 5 p. 443 - 452
反应条件
perchloric acid; pyridinium chlorochromate in water; acetic acid T=24.85 - 44.85°C; Oxidation; Kinetics;
参考文献
Kabilan; Girija; Rajagopal
International Journal of Chemical Kinetics, 1999 , vol. 31, # 10 p. 683 - 688
反应条件
perchloric acid; NaBO3; acetic acid T=24.9°C; var. temp., ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataMechanism;
参考文献
Kabilan, S.; Pandiarajan, K.; Krishnasamy, K.; Sankar, P.
International Journal of Chemical Kinetics, 1995 , vol. 27, # 5 p. 443 - 452
反应条件
1: 3-chlorobenzenethiol With sodium hydroxide in water
2: sodium salt of the chloroacetic acid in water
T=20°C; 4 h; Reflux;
3: With hydrogenchloride in water
T=20°C; pH=2;
参考文献
Okaecwe, Thokozile; Swanepoel, Abraham J.; Petzer, Anel; Bergh, Jacobus J.; Petzer, Jacobus P.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4336 - 4347
参考文献
Pasto,D.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2688 - 2691
反应条件
man fuehrt die gebildete Saeure in das Natriumsalz ueber und verkocht dieses mit Wasser;
参考文献
Friedlaender; Chwala; Slubek
Monatshefte fuer Chemie, 1907 , vol. 28, p. 251,273
反应条件
epoxysulfonyl fluoride
T=0°C;
参考文献
I.G. Farbenind.
Patent: DE464087 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 459