1-(3-羟基金刚烷-1-基)乙酮合成路线 (共 13 条)
参考文献
Daicel Chemical Industries, Ltd.
Patent: US6344590 B1, 2002 ;
Location in patent: Page column 26 ;
反应条件
ammonia; hydrogen; nickel in methanol T=100°C; P=71107.8 Torr; 6 h;
参考文献
Manchand; Cerruti; Martin; Hill; Merrett; Keech; Belshe; Connell; Sim
Journal of Medicinal Chemistry, 1990 , vol. 33, # 7 p. 1992 - 1995
反应条件
1: With sodium hydroxide; NaMnO4; water in tert-butyl alcohol T=30 - 40°C; 3.5 h; 2: With hydrogenchloride; water in isopropyl alcohol; tert-butyl alcohol Product distribution / selectivity;
参考文献
Williams, Eric L.
Patent: US2006/63950 A1, 2006 ;
Location in patent: Page/Page column 4 ;