反应条件
1.1: trichlorophosphate / 18 h / 0 - 20 °C / Inert atmosphere 1.2: 2 h / 0 - 20 °C / Inert atmosphere 2.1: triethylamine / methanol / 0.17 h / 20 °C / Inert atmosphere 2.2: 10 h / 150 °C / Inert atmosphere; Microwave irradiation 3.1: AlCl3, aluminium chloride; sodium azide / tetrahydrofuran / 18 h / Inert atmosphere; Reflux View Scheme
参考文献
Dolusic, Eduard; Larrieu, Pierre; Moineaux, Laurence; Stroobant, Vincent; Pilotte, Luc; Colau, Didier; Pochet, Lionel; Van Den Eynde, Benoit; Masereel, Bernard; Wouters, Johan; Frederick, Raphael
Journal of Medicinal Chemistry, 2011 , vol. 54, # 15 p. 5320 - 5334