(4-甲氧基苯乙炔基)三甲基硅烷合成路线 （共 73 条）
反应条件
toluene-4-sulfonic acid in neat (no solvent) T=60 - 140°C; 11 h; Green chemistry; regioselective reaction;
参考文献
Gao, Qi; Bao, Fang-Ping; Feng, Xiao-Jing; Pan, Ying-Ming; Wang, Heng-Shan; Li, Dian-Peng
Arkivoc, 2013 , vol. 2013, # 3 p. 49 - 60
反应条件
methanol; potassium carbonate in tetrahydrofuran T=20°C; 1 h; Inert atmosphere;
参考文献
Zhou, Ningzhang; Wang, Li; Thompson, David W.; Zhao, Yuming
Tetrahedron, 2011 , vol. 67, # 1 p. 125 - 143
反应条件
trichloroisocyanuric acid; water; silver nitrate in acetone T=0°C; Reflux;
参考文献
Synthesis, , # 9 art. no. T20708SS, p. 1469 - 1472
反应条件
dichloromethane; [Mo{(t-Bu)(3,5-dimethylphenyl)N}3] in toluene T=80°C;
参考文献
Fuerstner, Alois; Mathes, Christian
Organic Letters, 2001 , vol. 3, # 2 p. 221 - 223
反应条件
water; triethylamine; triphenylphosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=160°C; P=51485.6 Torr; 4 h;
参考文献
Takeuchi, Ryo; Yasue, Hiroyuki
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5386 - 5392
反应条件
1: methanol; potassium carbonate / dichloromethane / 2 h / 20 °C 2: Pd0(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)2; P[(2,6-OMe)2C6H3]3 / toluene / 5 h / 60 °C / Inert atmosphere View Scheme
参考文献
Jahier, Claire; Zatolochnaya, Olga V.; Zvyagintsev, Nickolay V.; Ananikov, Valentine P.; Gevorgyan, Vladimir
Organic Letters, 2012 , vol. 14, # 11 p. 2846 - 2849
反应条件
1: potassium carbonate / methanol / 3 h / 20 °C 2: carbonylchlorohydridetris(triphenylphosphine) ruthenium(II) / 0.5 h / 80 °C / |Inert atmosphere; |Microwave irradiation View Scheme
参考文献
Schabel, Tobias; Plietker, Bernd
Chemistry - A European Journal, 2013 , vol. 19, # 22 p. 6938 - 6941
反应条件
1: K2CO3 / methanol 2: N-methylpyrrolidine / RuCl2(=C=CHPh)(i-Pr3P)2 / CH2Cl2 / 5 h / 20 °C View Scheme
参考文献
Chemical Communications, , # 34 p. 4336 - 4338
反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere 2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 120 h / Inert atmosphere View Scheme
参考文献
Rassadin; Nicolas; Six
Chemical Communications, 2014 , vol. 50, # 57 p. 7666 - 7669
反应条件
copper(l) chloride in N,N-dimethyl-formamide T=80°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 39, # 23 p. 4075 - 4078
