六氢-1H-氮杂卓-4-醇合成路线 (共 3 条)
反应条件
1: With hydrogen; platinum(IV) oxide in methanol T=20°C; P=1125.11 Torr; 22 h; 2: in methanol T=20°C; 0.5 h;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; BOEHRINGER INGELHEIM PHARMA GMBH and CO. KG
Patent: WO2008/22979 A1, 2008 ;
Location in patent: Page/Page column 87 ;
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol 1 h; Heating / reflux;
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: EP1500643 A1, 2005 ;
Location in patent: Page 48 ;
EP 1500643 A1
反应条件
in dichloromethane T=20°C; 19 h;
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: EP1500643 A1, 2005 ;
Location in patent: Page 48 ;
EP 1500643 A1