1.1: sodium nitrite / water / 1.25 h / 0 - 5 °C / |Inert atmosphere
1.2: 1 h / 0 - 65 °C
1.3: 1 h / 40 - 50 °C
2.1: sodium acetate / acetonitrile / 0.5 h / 20 °C
2.2: 1 h / 0 - 5 °C
3.1: acetic acid / toluene / 1 h / |Reflux
View Scheme
参考文献
Shapiro, Rafael; DiCosimo, Robert; Hennessey, Susan M.; Stieglitz, Barry; Campopiano, Onorato; Chiang, George C.
Organic Process Research and Development, 2001 , vol. 5, # 6 p. 593 - 598
