1-(4-氟苯基)-4-硝基苯合成路线 （共 26 条）
反应条件
Ru/C; potassium hydroxide in ethanol; toluene T=120°C; 12 h; Microwave irradiation;
参考文献
Kim, Ju Hyun; Park, Ji Hoon; Chung, Young Keun; Park, Kang Hyun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2412 - 2418
反应条件
Ru/C; sodium hydroxide in tetrahydrofuran; ethanol T=105°C; 24 h; Microwave irradiation;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 13 p. 2412 - 2418
参考文献
van Hove
Bulletin de la Classe des Sciences, Academie Royale de Belgique, 1922 , vol. <5> 8, p. 507,527
Chem. Zentralbl., 1923 , vol. 94, # I p. 313
反应条件
C30H38Cl2N8Pd(2+)*2Cl(1-); tetrabutylammomium bromide; potassium carbonate in water
T=60°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Samarasimhareddy, Mamidi; Prabhu, Girish; Vishwanatha, Thimmalapura M.; Sureshbabu, Vommina V.
Synthesis (Germany), 2013 , vol. 45, # 9 p. 1201 - 1206
反应条件
Cell-OPPH2-Pd(0); potassium carbonate in ethanol; water
Suzuki-Miyaura reaction; 0.25 h; Reflux;
参考文献
Zhou, Bo; Li, Yi-Qun
E-Journal of Chemistry, 2011 , vol. 8, # 4 p. 1490 - 1497
反应条件
tetrabutyl ammonium fluoride; tri-cyclo-hexyl-phosphine; dichloro bis(acetonitrile) palladium(II)
T=85 - 90°C; Suzuki-Miyaura reaction; 5 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Xie, Ye-Xiang
Synthetic Communications, 2007 , vol. 37, # 14 p. 2433 - 2448
反应条件
1: 4-nitro-aniline With tetrafluoroboric acid; sodium nitrite in water
T=0 - 5°C; Diazotization; 0.5 h;
2: potassium (4-fluorophenyl)trifluoroborate With palladium diacetate in 1,4-dioxane
T=20°C; Arylation; 2.5 h;
参考文献
Darses, Sylvain; Michaud, Guillaume; Genet, Jean-Pierre
European Journal of Organic Chemistry, 1999 , # 8 p. 1875 - 1883
反应条件
1: p-fluorophenylgermanium trichloride With sodium hydroxide in 1,4-dioxane; water
T=20°C;
2: 1-bromo-4-nitro-benzene With palladium diacetate in 1,4-dioxane; water
1.5 h; Heating;
参考文献
Enokido, Tatsuki; Fugami, Keigo; Endo, Mayuko; Kameyama, Masayuki; Kosugi, Masanori
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1685 - 1688
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water
T=20°C; Suzuki-Miyaura cross-coupling; 3 h;
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
反应条件
dinitrogen tetraoxide in dichloromethane
48 h; Ambient temperature;
参考文献
Zhou, Li; Rajabzadeh, Masoumeh; Traficante, Daniel D.; Cho, Bongsup P.
Journal of the American Chemical Society, 1997 , vol. 119, # 23 p. 5384 - 5389
