2-甲氧基-4-硝基苯甲酰氯合成路线 （共 9 条）
反应条件
thionyl chloride
5 h; Reflux;
参考文献
ARES TRADING S.A.; QUATTROPANI, Anna; SWINNEN, Dominique
Patent: WO2013/182274 A1, 2013 ;
Location in patent: Page/Page column 46; 63 ;
反应条件
in N-methyl-acetamide; dichloromethane
参考文献
Pfizer Inc.
Patent: US4891372 A1, 1990 ;
反应条件
1: aqueous H2SO4 / anschliessendes Erwaermen mit wss. NaNO2
2: SOCl2
View Scheme
参考文献
Clinton et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 592,595
反应条件
1: aq.-ethanolic Na2CO3
2: SOCl2
View Scheme
参考文献
Clinton et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 592,595
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C / Inert atmosphere
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Adler, Marc J.; Hamilton, Andrew D.
Journal of Organic Chemistry, 2011 , vol. 76, # 17 p. 7040 - 7047
反应条件
1: 12 h / 20 °C
2: H2 / ethanol / 12 h / 20 °C
View Scheme
参考文献
Receveur, Jean-Marie; Bjurling, Emelie; Ulven, Trond; Little, Paul Brian; Norregaard, Pia K.; Hoegberg, Thomas
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 20 p. 5075 - 5080
反应条件
1: aqueous NaOH
2: FeSO4; aqueous NH3
View Scheme
参考文献
Backer; Houtman
Recueil des Travaux Chimiques des Pays-Bas, 1951 , vol. 70, p. 738,741
参考文献
Receveur, Jean-Marie; Bjurling, Emelie; Ulven, Trond; Little, Paul Brian; Norregaard, Pia K.; Hoegberg, Thomas
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 20 p. 5075 - 5080
参考文献
Adler, Marc J.; Hamilton, Andrew D.
Journal of Organic Chemistry, 2011 , vol. 76, # 17 p. 7040 - 7047
