1: methyl-phenyl-thioether With C30H21F6N2NiO2P in tetrahydrofuran
Schlenk techniqueInert atmosphere;
2: 2-Bromo-1,3,5-trimethyl-benzene With magnesium; lithium chloride in tetrahydrofuran
T=70°C; 24 h;
参考文献
Someya, Chika I.; Weidauer, Maik; Enthaler, Stephan
Catalysis Letters, 2013 , vol. 143, # 5 p. 424 - 431
Hey
Journal of the Chemical Society, 1932 , p. 2636,2638
Full Text Show Details
Grieve; Hey
Journal of the Chemical Society, 1934 , p. 1797,1798,1802
Journal of the Chemical Society, 1938 , p. 108,110
hydrogenchloride
Diazotization.Behandlung der Diazoniumsalz-Loesung mit Benzol in Gegenwart von MgSO4 bei 0grad bis 5grad und Versetzen des Reaktionsgemisches mit konz. wss. NaOH;
参考文献
Hey
Journal of the Chemical Society, 1932 , p. 2636,2638
Hey
Journal of the Chemical Society, 1932 , p. 2636,2638
Full Text Show Details
Grieve; Hey
Journal of the Chemical Society, 1934 , p. 1797,1798,1802
Journal of the Chemical Society, 1938 , p. 108,110