2-[(4-氯苯甲酰基)氨基]乙酸乙酯合成路线 （共 14 条）
反应条件
potassium hydroxide in ethanol T=20°C; 0.5 h;
参考文献
Pessoa-Mahana, Hernan; Astudillo, Claudio I. O.; Araya-Maturana
Synthetic Communications, 2002 , vol. 32, # 9 p. 1437 - 1445
反应条件
1: sodium hydride; 18-crown-6 ether / toluene / 3 h / 20 - 60 °C / |Cooling with ice 2: Lawesson's reagent / 1,4-dioxane / 12 h / |Reflux View Scheme
参考文献
Khose, Goraksha; Shinde, Shailesh; Panmand, Anil; Kulkarni, Ravibhushan; Munot, Yogesh; Bandyopadhyay, Anish; Barawkar, Dinesh; Patil, Santoshkumar N.
Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2671 - 2674
反应条件
1: sodium hydride; 18-crown-6 ether / toluene / 3 h / 20 - 60 °C / |Cooling with ice
2: triethylamine; triphenylphosphine; iodine / dichloromethane / 3 h / 20 °C
View Scheme
参考文献
Khose, Goraksha; Shinde, Shailesh; Panmand, Anil; Kulkarni, Ravibhushan; Munot, Yogesh; Bandyopadhyay, Anish; Barawkar, Dinesh; Patil, Santoshkumar N.
Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2671 - 2674
反应条件
potassium hydroxide; hydroxylamine hydrochloride in methanol
Ambient temperature; Yield given;
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
