1: 90 percent / I2, P(red) / toluene / 8 h / Heating 2: 67 percent / KOH / methanol / 4 h / Heating 3: 76 percent / toluene / 12 h / 60 °C 4: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 5: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Groesbeek, M.; Galen, A. J. J. van; Ippel, J. H.; Berden, J. A.; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1993 , vol. 112, # 4 p. 237 - 246
1: H2 / 15percent Ni/SiO2 / 230 - 240 °C / 26252.1 - 30002.4 Torr / flow unit, 0.25 h-1 space velocity
2: LiAlH4
View Scheme
参考文献
Kozintsev, S. I.; Zhavrid, A. S.; Serzhanin, A. I.; Kozlov, N. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 12 p. 1346 - 1348
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 12 p. 1619 - 1622
Kozintsev, S. I.; Zhavrid, A. S.; Serzhanin, A. I.; Kozlov, N. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 12 p. 1346 - 1348
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 12 p. 1619 - 1622
Groesbeek, M.; Galen, A. J. J. van; Ippel, J. H.; Berden, J. A.; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1993 , vol. 112, # 4 p. 237 - 246
