4-乙酰氧基-3,5-二甲氧基苯甲酰氯合成路线 （共 16 条）
反应条件
1: palladium/BaSO4; xylene / Hydrogenation 2: pyridine; aniline; piperidine View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: 30 percent / 1.) pyridine, 2.) water / benzene / Heating; 1.) 15 min, 2.) 15 min 2: 0.2 M aq. NaOH / ethanol / 0.25 h / Ambient temperature View Scheme
参考文献
Jogia, Madhu K.; Vakamoce, Veikila; Weavers, Rex T.
Australian Journal of Chemistry, 1985 , vol. 38, # 7 p. 1009 - 1016
反应条件
1: diazomethane / diethyl ether / -5 - 0 °C 2: ammonium acetate / water; methanol / 8 h / 50 °C 3: water; biphenyl / acetonitrile / 0.13 h / |Irradiation View Scheme
参考文献
Senadheera, Sanjeewa N.; Evans, Anthony S.; Toscano, John P.; Givens, Richard S.
Photochemical and Photobiological Sciences, 2014 , vol. 13, # 2 p. 324 - 341
反应条件
1: palladium/BaSO4; xylene / Hydrogenation 2: aniline; pyridine 3: pyridine; SOCl2 4: palladium/BaSO4; dioxane; quinoline / Hydrogenation.Reagens 4:Xylol;Behandeln des Reaktionsprodukts in CHCl3 mit Natriummethylat in Methanol View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: palladium/BaSO4; xylene / Hydrogenation 2: CHCl3; methanol. sodium methylate 3: palladium/BaSO4; acetic acid / Hydrogenation View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
Pd-BaSO4; xylene Hydrogenation;
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: pyridine / benzene / 18 h / 25 °C 2: NaH / dimethylsulfoxide / 1.5 h / 60 °C 3: 178 mg / H2SO4 / Heating View Scheme
参考文献
Kuwabara, Hidenori; Mouri, Kyoko; Otsuka, Hideaki; Kasai, Ryoji; Yamasaki, Kazuo
Journal of Natural Products, 2003 , vol. 66, # 9 p. 1273 - 1275
反应条件
Pd-BaSO4; xylene T=150 - 160°C; Hydrogenation;
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: palladium/BaSO4; xylene / Hydrogenation 2: CHCl3; methanol. sodium methylate View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: palladium/BaSO4; xylene / Hydrogenation 2: aniline; pyridine View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
